Triphenyl phosphate synthesis
- Product Name:Triphenyl phosphate
- CAS Number:115-86-6
- Molecular formula:C18H15O4P
- Molecular Weight:326.28
101-02-0
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115-86-6
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Triphenyl Phosphate (Table 2, Entry 1); Typical Procedure
General procedure: A solution of (PhO)3P (0.0773 g, 0.250 mmol) in (bmim)[PF6] (5mL) containing 5 (0.0330 g, 0.0500 mmol) and rose bengal(0.0128 g, 0.0125 mmol) was vigorously stirred in an open flaskand irradiated with a 60 W LED lamp for 2.5 h. The temperaturewas kept at about 15 °C by using an ice bath during the irradiation.The resulting mixture was extracted with Et2O, and thesolvent was then evaporated to give a pink solid; yield: 0.0803 g(99%); mp 44-47 °C.1H NMR (500 MHz, CDCl3): = 7.36 (t, J = 7.7, 6 H), 7.25-7.19(m, 9 H). 13C NMR (125 MHz, CDCl3): = 150.6, 150.5, 130.0,125.7, 120.3, 120.2. 31P NMR (202 MHz, CDCl3): = -17.7. HRMS(APCI): m/z [M + H]+ calcd for C18H16O4P: 327.0781; found:327.0743.
2524-64-3
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108-95-2
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115-86-6
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108-95-2
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115-86-6
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135-19-3
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108-95-2
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115-86-6
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18872-49-6
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